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DOI10.3390/ma12060911
Room temperature synthesis of V-Doped TiO2 and its photocatalytic activity in the removal of caffeine under UV Irradiation
Sacco O.; Sannino D.; Matarangolo M.; Vaiano V.
发表日期2019
ISSN19961944
卷号16期号:6
英文摘要In this work, the influence of simple acids in the room temperature sol-gel synthesis of TiO2 was investigated and the efficiency of prepared photocatalysts was evaluated in the removal of caffeine. To improve the photoactivity of TiO2, vanadium-doped TiO2 (VTiO2) samples were obtained starting from different amount of vanadyl sulphate as a dopant source. The samples were centrifuged, washed and finally dried at room temperature, and no calcination step was carried out. The prepared photocatalysts were characterized by different techniques (X-ray powder diffraction (XRD), specific surface area (SSA), ultraviolet-visible diffuse reflectance spectra (UV-vis DRS) and Raman). VTiO2 photocatalysts were tested in the photocatalytic removal of aqueous solutions containing caffeine. The photocatalytic tests were carried out in a recirculating batch cylindrical photoreactor irradiated by a UV LEDs strip (nominal power of 12 W and wavelength emission peak at about 365 nm) surrounding the external surface of the reactor. The optimized VTiO2 photocatalyst was able to reach a caffeine degradation of about 96% after 360 min of UV light irradiation with a total organic carbon (TOC) removal of 72%. by the authors. Licensee MDPI, Basel, Switzerland.
英文关键词Caffeine; Photocatalysis; Roomtemperature synthesis; Sol-gel; V-doped TiO2; Water treatment
scopus关键词Irradiation; Organic carbon; Photocatalysis; Photocatalytic activity; Sol-gel process; Sol-gels; Sulfur compounds; Titanium dioxide; Vanadium compounds; Water treatment; X ray powder diffraction; Caffeine degradations; Diffuse reflectance spectrum; Photo-catalytic removal; Room temperature synthesis; Sol - Gel synthesis; Specific surface area (SSA); Total Organic Carbon; UV-light irradiation; Caffeine
来源期刊Materials
文献类型期刊论文
条目标识符http://gcip.llas.ac.cn/handle/2XKMVOVA/176480
作者单位Department of Industrial Engineering, University of Salerno, Via Giovanni Paolo II 132, Fisciano (SA), 84084, Italy
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Sacco O.,Sannino D.,Matarangolo M.,et al. Room temperature synthesis of V-Doped TiO2 and its photocatalytic activity in the removal of caffeine under UV Irradiation[J],2019,16(6).
APA Sacco O.,Sannino D.,Matarangolo M.,&Vaiano V..(2019).Room temperature synthesis of V-Doped TiO2 and its photocatalytic activity in the removal of caffeine under UV Irradiation.Materials,16(6).
MLA Sacco O.,et al."Room temperature synthesis of V-Doped TiO2 and its photocatalytic activity in the removal of caffeine under UV Irradiation".Materials 16.6(2019).
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